: Place the prepared sample evenly on the sample stage, ensuring that the sample surface is flat and perpendicular to the incident X-ray beam to guarantee the accuracy of the diffraction data.

: Start the X-ray diffractometer and scan according to the set parameters. During the scan, the diffractometer will automatically record the diffraction intensities at different angles and generate a diffraction pattern.

 

 

 

: If it is necessary to further determine the content of the brittle phases, various quantitative analysis methods can be adopted, such as the internal standard method, external standard method, K-value method, etc. These methods require the measurement of the diffraction peak intensities of the sample and the standard sample on the basis of known standard samples, and then calculate the content of the brittle phases in the sample by combining the corresponding calculation formulas.

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